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Thermo-responsive assembly of 60-AuND-(97:3): ( a ) the extinction spectra of 60-AuND-(97:3) upon heating from 25 to 70 °C and ( b ) upon cooling from 70 to 25 °C; ( c ) the extinction values at 715 nm against temperature changes; ( d ) the reversible changes in extinction values between 25 and 70 °C. The red arrows in ( a , b ) indicate the plasmon peak changes.

Journal: Nanomaterials

Article Title: Hysteresis in the Thermo-Responsive Assembly of Hexa(ethylene glycol) Derivative-Modified Gold Nanodiscs as an Effect of Shape

doi: 10.3390/nano12091421

Figure Lengend Snippet: Thermo-responsive assembly of 60-AuND-(97:3): ( a ) the extinction spectra of 60-AuND-(97:3) upon heating from 25 to 70 °C and ( b ) upon cooling from 70 to 25 °C; ( c ) the extinction values at 715 nm against temperature changes; ( d ) the reversible changes in extinction values between 25 and 70 °C. The red arrows in ( a , b ) indicate the plasmon peak changes.

Article Snippet: The following supporting information can be downloaded at: https://www.mdpi.com/article/10.3390/nano12091421/s1 , Scheme S1: Illustration of AuND synthesis; Figure S1: Characterization of gold nanotriangles (AuNTs); Figure S2: A plot of the zeta potential of AuNDs against the COOH content; Figure S3: Thermo-responsive assembly of 105-AuND-(100:0); Figure S4: SEM and STEM images of 105-AuND-(97:3) dried at 25 and 60 °C; Figure S5: Salt-induced assembly of 105-AuND-(97:3); Figure S6: Thermo-responsive assembly of 60-AuND-(100:0); Figure S7: Characterization of 40-AuNSs; Figure S8: Thermo-responsive behavior of 40-AuNS-(99:1); Figure S9: Thermo-responsive assembly of 105-AuND-(99:1); Figure S10: Thermo-responsive assembly of 105-AuND-(95:5); Figure S11: Thermo-responsive behavior of 105-AuND-(90:10); Figure S12: Thermo-responsive assembly of 60-AuND-(99:1); Figure S13: Thermo-responsive assembly of 60-AuND-(95:5); Figure S14: Thermo-responsive behavior of 60-AuND-(90:10); Figure S15: Effects of COOH content and zeta potential on assembly temperature of 60-AuNDs; Figure S16: A plot of the changes in extinction during the time course experiment at 25, 40, 45, 50, 55, and 60 °C; Figure S17: Thermo-responsive assembly of 60-AuND-(97:3) with 30 min of waiting time; Figure S18: The degree of hysteresis with the 5 and 30 min waiting time for 60-AuND-(99:1).

Techniques:

Rate-independent hysteresis of 60-AuND-(97:3): ( a ) the extinction values at 715 nm against temperature changes with a 30 min waiting time for 60-AuND-(97:3); ( b ) a plot of the degree of hysteresis during 5 and 30 min waiting times for 60-AuND-(97:3). The error bars represent standard deviation of the mean ( n = 3).

Journal: Nanomaterials

Article Title: Hysteresis in the Thermo-Responsive Assembly of Hexa(ethylene glycol) Derivative-Modified Gold Nanodiscs as an Effect of Shape

doi: 10.3390/nano12091421

Figure Lengend Snippet: Rate-independent hysteresis of 60-AuND-(97:3): ( a ) the extinction values at 715 nm against temperature changes with a 30 min waiting time for 60-AuND-(97:3); ( b ) a plot of the degree of hysteresis during 5 and 30 min waiting times for 60-AuND-(97:3). The error bars represent standard deviation of the mean ( n = 3).

Article Snippet: The following supporting information can be downloaded at: https://www.mdpi.com/article/10.3390/nano12091421/s1 , Scheme S1: Illustration of AuND synthesis; Figure S1: Characterization of gold nanotriangles (AuNTs); Figure S2: A plot of the zeta potential of AuNDs against the COOH content; Figure S3: Thermo-responsive assembly of 105-AuND-(100:0); Figure S4: SEM and STEM images of 105-AuND-(97:3) dried at 25 and 60 °C; Figure S5: Salt-induced assembly of 105-AuND-(97:3); Figure S6: Thermo-responsive assembly of 60-AuND-(100:0); Figure S7: Characterization of 40-AuNSs; Figure S8: Thermo-responsive behavior of 40-AuNS-(99:1); Figure S9: Thermo-responsive assembly of 105-AuND-(99:1); Figure S10: Thermo-responsive assembly of 105-AuND-(95:5); Figure S11: Thermo-responsive behavior of 105-AuND-(90:10); Figure S12: Thermo-responsive assembly of 60-AuND-(99:1); Figure S13: Thermo-responsive assembly of 60-AuND-(95:5); Figure S14: Thermo-responsive behavior of 60-AuND-(90:10); Figure S15: Effects of COOH content and zeta potential on assembly temperature of 60-AuNDs; Figure S16: A plot of the changes in extinction during the time course experiment at 25, 40, 45, 50, 55, and 60 °C; Figure S17: Thermo-responsive assembly of 60-AuND-(97:3) with 30 min of waiting time; Figure S18: The degree of hysteresis with the 5 and 30 min waiting time for 60-AuND-(99:1).

Techniques: Standard Deviation